Application / Catalyst Recovery

Your catalyst is worth more than the batch. Stop losing it to the filter.

Closed-circuit recovery systems on in-house Clarysynt sintered metal: up to 99 percent single-pass recovery of palladium, platinum, rhodium, and Raney nickel, with elements that regenerate in place for thousands of batches.

Photograph to shoot
Complete catalyst recovery skid in the assembly bay: candle housing, backwash manifold, PLC panel. Engineer at the panel for scale.
The problem, in your process terms
Customer processHydrogenation and debenzylation in API and fine chemical synthesis, H2O2 production, edible oil hardening, refinery slurry duty
Critical problemPrecious metal leaving with the filtrate or the cake, open handling of pyrophoric catalyst, filter aid consumption, batch time lost to recirculation
Engineering solutionAsymmetric dual-layer Clarysynt sintered elements in a closed, automated circuit with reverse-flow backwash and integrated heel filtration
EvidenceUp to 99% single-pass recovery, 0.5 micron fines capture, elements in continuous service beyond 5,000 batches (duty and maintenance dependent), bench and pilot trial data on your own slurry before purchase
Engineering envelope
RecoveryUp to 99% precious metal recovery, single pass
Retention ratings0.5 to 25 micron, matched to catalyst particle size distribution
Flow capacityUp to 1,500 m3/hr in a single housing, subject to engineering review; multi-housing skids for higher flows
TemperatureCryogenic (minus 150 C) to 900 C, alloy and seal dependent, subject to engineering review
MaterialsSS 316L standard; SS 304, Hastelloy C-276, Inconel 600, Monel 400, Titanium, Zirconium for aggressive service
Design codesASME Section VIII, PED, or IBR as required
OperationFully closed circuit, automated PLC or DCS control, integrated heel filter for complete liquid recovery
RegenerationAutomated reverse-flow gas or liquid backwash; element design life up to 10 years or more, depending on duty, cleaning protocol and operation
Element dimensionsOD 25 mm to 60 to 75 mm, lengths 250 to 1,500 mm; custom OD and lengths on request
Element structureSintered metal powder; asymmetric dual-layer construction for fine ratings, with a thin active layer of about 200 micron on a coarser carrier
Control panelFlameproof for Zone 1 and 2 or non-flameproof for safe areas; ATEX and IECEx options available
ValvesPneumatic or electric actuation; butterfly or ball valves per application

Datasheets, application notes, and cleaning protocols are available on request.

Catalysts we recover, by name
CatalystTypical duty
Palladium on carbon (Pd/C)Hydrogenation, debenzylation in API synthesis
Platinum on carbon (Pt/C)Selective hydrogenation, fine chemicals
Rhodium on carbon (Rh/C)Specialty hydrogenation duty
Ruthenium catalystsFine chemical and specialty synthesis
Raney nickelPyrophoric: closed-circuit nitrogen-blanketed handling as standard
FCC catalyst finesRefinery slurry and fines recovery
Platinum oxide (PtO2)Pharmaceutical hydrogenation and reduction
Palladium in H2O2 productionWorking solution filtration after the hydrogenation stage of the anthraquinone process; primary plus polishing stages typical
Ni/Mo, Co/Mo and Pt/Re catalystsHydrocracking catalyst recovery, reforming catalyst filtration
Supported nickelEdible oil hardening; food-grade SS 316L, closed circuit for nickel safety
How an engagement runs

From your slurry sample to a running system.

Feasibility and bench trials

Your slurry, our lab. Retention, flux, and cake behaviour established before any steel is cut.

Pilot systems

Skid-mounted pilot units prove recovery and cycle times on your line before scale-up.

Engineering and fabrication

P&ID and process design through ASME Section VIII, PED, or IBR coded fabrication as required, with PLC or DCS automation.

Commissioning and support

Installation, cycle tuning, operator training, and element regeneration support for the life of the system.

Three ways in

New system, retrofit, or replacement elements?

Drop-in element replacement

Sintered elements made to the dimensions, end connections and seal configuration of the candles already in your housings. The fastest route, with no change to the vessel.

Full retrofit

A closed sintered metal system in place of sparkler, plate-and-frame, Nutsche or bag filtration, returning catalyst to the reactor instead of sending it out on pads.

New system supply

Skid-mounted or field-erected: filter vessels and elements, integrated heel filter, piping, valves and instruments, flameproof or safe-area PLC panel, nitrogen blanketing, P&ID integration and installation supervision.

For consultants and EPC teams

Process data review, sizing calculations, element and material selection, P&ID integration review, and budget pricing for feasibility studies and DFR submissions.

Before it ships

What is tested, element by element and system by system?

  • Raw material: alloy powder composition by spectrometric analysis, particle size distribution, material test certificate for every lot
  • Element: integrity test by bubble point or diffusion, dimensional inspection, micron rating verification of largest and average pore size, permeability test
  • Special alloys: corrosion resistance testing; periodic ultrasonic testing for fatigue resistance
  • System: hydrostatic test to the design code, NDE of pressure-retaining welds by radiography, UT or dye penetrant as applicable, functional test of the automation sequence
  • Documents: material test certificates, weld maps, NDE reports and pressure test certificates

Who makes the candles in your catalyst system?

At Gopani, we do. In-house Clarysynt media means your recovery rate, your spare elements, and your custom geometries are engineered and manufactured in Ahmedabad, at Indian lead times and INR pricing, with media manufacture and system engineering in one company.

Pharmaceutical or API manufacturer? Read the pharma page.

How much catalyst does the system actually recover?

Up to 99 percent single-pass recovery of precious metal catalyst, using asymmetric dual-layer Clarysynt sintered elements as a positive surface barrier. Single-pass operation matters: it eliminates the multi-pass recirculation that older systems rely on, which shortens batch time and reduces catalyst attrition. For your specific slurry we establish the recovery figure in a bench or pilot trial before you commit.

How does this compare with sparkler filters or centrifuges?

Sparkler filters and open filtration steps expose the batch and the operators, lose fines below their retention capability, and consume filter aids and cloths every cycle. A closed sintered-metal circuit captures fines down to 0.5 micron, recovers the heel through an integrated heel filter, needs no filter aids, and returns the same elements to service for thousands of batches. The saving is counted in recovered metal, not in filter spend.

Can it handle Raney nickel safely?

Yes. Raney nickel duty runs as a fully closed circuit under nitrogen blanketing, with no atmospheric exposure of the pyrophoric catalyst at any point in the cycle, including cake discharge. Safety interlocks are engineered into the automation, not left to procedure.

What does maintenance look like over the years?

Elements regenerate in place by reverse-flow gas or liquid backwash on an automated cycle. Design life is up to 10 years or more per element set; some elements in continuous service have run beyond 5,000 batches. Actual life depends on the process fluid, catalyst, temperature, cleaning protocol and operator discipline. Because Clarysynt media is manufactured in-house in Ahmedabad, replacement elements and rebuild support do not wait on an import.

How much is catalyst loss costing us today?

At 200 hydrogenation batches a year, losing 2 percent of a Pd/C charge per batch adds up to tens of lakhs of rupees a year in metal alone, before the reactor hours lost to multi-pass filtration and the disposal of catalyst-laden pads as hazardous waste. The number depends on your loading and the metal price, so we calculate it from your batch record.

Can you replace sintered candles already installed in our housings?

Yes. We make drop-in replacement elements for sintered metal candles from other manufacturers, matching dimensions, end connections and seal configuration, so they fit the existing housing. Where the fine-rating dual-layer construction applies, lower differential pressure means less mechanical stress on the catalyst and less attrition into fines.

Which alloy for corrosive or high-temperature service?

SS 316L is standard, with SS 304 where it suits. Hastelloy C-276 for strong acids and chloride environments, Inconel 600 for high-temperature oxidising service, Monel 400 for reducing environments, titanium for strong oxidising acids, and zirconium for sulfuric acid service. Send the process fluid, temperature and pressure for a recommendation.

How does catalyst recovery work in H2O2 production?

In the anthraquinone process a palladium catalyst is suspended in the working solution during hydrogenation and must be separated before the oxidation stage. A sintered metal system captures the catalyst in a single pass, backwashes it for reuse, and passes clear working solution forward; a primary plus polishing arrangement is typical for the filtrate clarity H2O2 plants need.

What is the lead time for a system or replacement elements?

Element replacements are typically quoted at 6 to 8 weeks, standard-design systems at 8 to 10 weeks, and custom-engineered systems with special alloys, large sizes or code-stamped vessels at 8 to 12 weeks. The lead time for your order is confirmed with the quotation.

Do you supply outside India?

Yes. Sintered metal elements and catalyst recovery systems have been exported to customers in the USA, Europe, the Middle East, Africa, Southeast Asia and Australia, with export documentation and sea or air freight packing.

Send one batch record.

Catalyst type, loading, solvent, temperature, and batch size. We will estimate the recoverable value you are currently losing and propose the trial that proves it.